November 2023

Journal

POWGEN: rebuild of a third-generation powder diffractometer at the spallation neutron source

By:
Huq, Ashfia ; Kirkham, Melanie J; Peterson, Peter F; Hodges, Jason P; Whitfield, Pamela S; Page, Katharine L; Huegle, Thomas ; Iverson, Erik B; Parizzi, Andre D; Rennich, George Q
Journal Name:
Journal of Applied Crystallography
Page Number:
1-13
Volume:
52
Issue Number:
5
Publication Date:
November 9, 2023
View DOI Listing:
https://doi.org/10.1107/S160057671901121X

Abstract

The neutron powder diffractometer POWGEN at the Spallation Neutron Source has recently (2017–2018) undergone an upgrade which resulted in an increased detector complement along with a full overhaul of the structural design of the instrument. The current instrument has a solid angular coverage of 1.2 steradians and maintains the original third-generation concept, providing a single-histogram data set over a wide d-spacing range and high resolution to access large unit cells, detailed structural refinements and in situ/operando measurements.